| 研究生: |
蘇裕展 Su, Yu-Chan |
|---|---|
| 論文名稱: |
灌膠製程環氧樹脂乾固品質評估方法 Assessment Method for Epoxy Resin Curing Quality in Potting Processes |
| 指導教授: |
陳建富
Chen, Jiann-Fu 羅國原 Lo, Kuo-Yuan |
| 學位類別: |
碩士 Master |
| 系所名稱: |
電機資訊學院 - 電機工程學系 Department of Electrical Engineering |
| 論文出版年: | 2026 |
| 畢業學年度: | 114 |
| 語文別: | 中文 |
| 論文頁數: | 81 |
| 中文關鍵詞: | 灌膠製程 、環氧樹脂 、介質損耗角 、局部放電 、介電指標 、乾固品質 |
| 外文關鍵詞: | Potting Process, Epoxy Resin, Dissipation Factor, Partial Discharge, Dielectric Degradation Indicator, Curing Quality |
| 相關次數: | 點閱:3 下載:0 |
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研究旨在探討介質損耗角量測應用於灌膠製程環氧樹脂乾固品質評估之可行性,並與局部放電(PD)量測結果進行比較分析。局部放電量測可有效反映材料內部缺陷,而介質損耗角量測則可藉由材料介電特性變化評估其乾固狀態與絕緣品質。
研究以一般環境灌膠與真空灌膠兩種製程條件製備環氧樹脂試片,分別進行局部放電與介質損耗角量測。結果顯示,真空灌膠試片具有較低之局部放電幅值,且介電指標(DI)多呈負值;相較之下,一般環境灌膠試片之局部放電幅值較高,且 DI 值多呈正值,顯示其介電損耗與放電風險較高。
綜合分析結果可知,介質損耗角量測所建立之 DI 指標與局部放電量測結果呈現一致之品質判別趨勢,能有效區分不同灌膠製程下之乾固品質差異。研究結果顯示,介質損耗角量測與局部放電量測皆具有良好的品質辨識能力,可依不同檢測需求與應用情境作為環氧樹脂灌膠品質評估之工具。
This study investigates the feasibility of using dielectric loss tangent measurements to evaluate the curing quality of epoxy resin in potting processes and compares the results with partial discharge (PD) measurements. PD measurements are commonly used to detect internal insulation defects, whereas dielectric loss tangent measurements evaluate insulation quality through changes in dielectric properties.
Epoxy resin specimens were prepared using atmospheric potting and vacuum potting processes. The results showed that vacuum-potted specimens exhibited lower PD amplitudes and lower dielectric degradation index (DI) values, indicating better insulation quality. In contrast, atmospheric-potted specimens exhibited higher PD amplitudes and higher DI values, suggesting greater dielectric loss and discharge risk.
The results demonstrate that the DI index derived from dielectric loss tangent measurements shows a quality assessment trend consistent with PD measurements and can effectively distinguish curing quality differences between potting processes. Therefore, both dielectric loss tangent and PD measurements can serve as effective methods for evaluating the curing quality of epoxy resin under different testing requirements and application scenarios.
[1] IEC, IEC 60270: High-voltage test techniques – Partial discharge measurements, Edition 3.1, 2015.
[2] IEEE Standards Association, The Authoritative Dictionary of IEEE Standards Terms, IEEE Std 100-2000, 2000.
[3] M. Ghaffarian Niasar, "Partial Discharge Signatures of Defects in Insulation Systems Consisting of Oil and Oil-Impregnated Paper," KTH Royal Institute of Technology, 2012.
[4] 黃冠霖,「油浸式變壓器絕緣紙劣化診斷研究」, 2025 年。
[5] X. Lu, K. Hou, Q. Li, W. Si, and C. Fu, "Statistical Analysis and Discharge Type Identification of Partial Discharge Pulse Parameters of Oil-Paper Insulation Based on Ultra-wideband," in 2021 International Conference on Advanced Electrical Equipment and Reliable Operation (AEERO), 2021: IEEE, pp. 1-6.
[6] F. Kreuger, E. Gulski, and A. Krivda, "Classification of Partial Discharges," IEEE transactions on Electrical Insulation, vol. 28, no. 6, pp. 917-931, 1993.
[7] 陳建富,「模鑄型變壓器部分放電之音射檢測法」,行政院國家科學委員會電力科技產業學術合作研究計畫,1998 年。
[8] F. H. Kreuger, Partial discharges in electrical power apparatus, Butterworths, London, UK, 1989.
[9] E. Gulski and F. H. Kreuger,"Computer-aided recognition of discharge sources,"
IEEE Transactions on Electrical Insulation,vol. 27, no. 1, pp. 82-92, 1992.
[10] X. Liu, P. Lan, and N. Lin, “Curing reactions of epoxy powder coatings in perspectives of chemical mechanisms and strategies,” Progress in Organic Coatings, vol. 199, p. 108956, 2025.
[11] C. A. May,epoxy resins: chemistry and technology,2nd ed., Marcel Dekker, New York, USA, 1988.
[12] H. Zhu, Y. Wang, H. Fu, Y. Liang, S. Sheng, T. Li, T. Wang, Y. Wang, and H. Sun, “The effect of epoxy resin and curing agent groups on the bonding properties of structural adhesives,” Results in Materials, vol. 24, p. 100540, 2024.
[13] S. R. Mousavi, S. Estaji, H. Kiaei, M. Mansourian-Tabaei, S. Nouranian, S. H. Jafari, H. Ruckdäschel, M. Arjmand, and H. A. Khonakdar, “A review of electrical and thermal conductivities of epoxy resin systems reinforced with carbon nanotubes and graphene-based nanoparticles,” Polymer Testing, vol. 112, p. 107645, 2022.
[14] J. D. Lee and T. C. Wei,"Properties and applications of bisphenol-F epoxy resins in electrical insulation systems,"Journal of Applied Polymer Science, vol. 120, no. 3, pp. 1452–1460, 2011.
[15] R. Hardis, J. L. P. Jessop, F. E. Peters, and M. R. Kessler, “Cure kinetics characterization and monitoring of an epoxy resin using DSC, Raman spectroscopy, and DEA,” Composites Part A: Applied Science and Manufacturing, vol. 49, pp. 100–108, 2013.
[16] D. Abraham, G. McIlhagger, and G. P. McIlhagger, “Glass fibre epoxy composite cure monitoring using parallel dielectric analysis and raman spectroscopy,” Composites Part A: Applied Science and Manufacturing, vol. 29, no. 7, pp. 815–819, 1998.
[17] S. Z. L. Htet, T. Kondo, T. Miyake, T. Sakoda, and T. Nishimura, “Partial discharge behavior prior to breakdown in epoxy resin containing insulation paper with a void defect,” Electrical Engineering in Japan, 2024.
[18] M. Mehdikhani, L. Gorbatikh, I. Verpoest, and S. V. Lomov, “Voids in fiber-reinforced polymer composites: A review on their formation, characteristics, and effects on mechanical performance,” Journal of Composite Materials, vol. 53, no. 12, pp. 1579–1669, 2019.
[19] S. C. Garcea, Y. Wang, and P. J. Withers, “X-ray computed tomography of polymer composites,” Composites Science and Technology, vol. 156, pp. 305–319, 2018.
[20] A. Kyriazis, T. Andritsch, and P. H. F. Morshuis, “Comparison of different cure monitoring techniques,” Sensors, vol. 22, no. 19, 7301, 2022.
[21] F. Álvarez, F. Garnacho, J. Ortego, and M. Á. Sánchez-Urán, “Application of HFCT and UHF sensors in on-line partial discharge measurements for insulation diagnosis of high voltage equipment,” Sensors, vol. 15, no. 4, pp. 7360–7387, 2015.
[22] G. Akbar, S. Islam, and M. S. J. Singh, “A detailed review of partial discharge detection methods for sic power modules under square-wave voltage excitation,” Energies, vol. 17, no. 22, 5793, 2024.
[23] Z. Wu et al., “In situ monitoring of epoxy resin curing process,” Polymer Testing, 2023.
[24] L. Du et al., “Equivalence analysis of dielectric test methods in time and frequency domains,” Cryogenics, 2025.
[25] A. Krotowski et al., “Analysis of polarization and depolarization currents…,” Energies, 2022.
[26] I. Fofana et al., “Low temperature and moisture effects on polarization…,” Electric Power Systems Research, 2010.
[27] S. Kaziz, M. H. Said, A. Imburgia, B. Maamer, D. Flandre, P. Romano, and F. Tounsi, "Radiometric partial discharge detection: A review," Energies, vol. 16, no. 6, pp. 2712, 2023.
[28] H. Song, G. J. Pundareekam, J. Ye, W. Jung, J. Ji, and J. Ryu, “Review of the thermally stimulated depolarization current (TSDC) technique for characterizing dielectric materials,” Journal of the Korean Ceramic Society, vol. 60, no. 5, pp. 747–759, 2023, doi: 10.1007/s43207-023-00305-5.
[29] T. K. Saha, "Review of modern diagnostic techniques for assessing insulation condition in aged transformers," IEEE Transactions on Dielectrics and Electrical Insulation, vol. 10, no. 5, pp. 903-917, Oct. 2003.
[30] W. S. Zaengl, "Dielectric spectroscopy in time and frequency domain for HV power equipment, part I: theoretical considerations," IEEE Electrical Insulation Magazine, vol. 19, no. 5, pp. 5–19, Sep.–Oct. 2003.
[31] HFCT 48 Product Specification, IPEC. [Online]. https://ipecuk.com/our-products/hfct/ (accessed 2025).
[32] G. Luo and D. Zhang, "Study on performance of developed and industrial HFCT sensors," in 2010 20th Australasian Universities Power Engineering Conference, 2010: IEEE, pp. 1-5.
[33] X. Hu, W. H. Siew, M. D. Judd, and X. Peng, “Transfer function characterization for HFCTs used in partial discharge detection,” in IEEE Transactions on Dielectrics and Electrical Insulation, Vol. 24, No. 2, pp. 1088-1096, April 2017.
[34] P. Technology. "Pico technology: PC oscilloscope, data logger & RF products." https://www.picotech.com/ (accessed.2025.
[35] HIOKI E.E. Corporation, LCR Meter IM3533 Product Page / Specifications, available from HIOKI official website.
[36] Westlake Epoxy, “Technical data sheet EPON™ Resin 862,” 2005.
[37] Everchem Specialty Chemicals, “Safety data sheet YDF 170,” 2021.
[38] Kukdo Chemical, “EPOKUKDO YDF-170 technical data sheet.”