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研究生: 劉柏志
Liu, Po-Chih
論文名稱: 7075與A356鋁合金異質摩擦攪拌銲接後之微觀組織及拉伸性質研究
Microstructure and Tensile Properties of Dissimilar Friction Stir Welded 7075 and A356 Aluminum Alloys
指導教授: 呂傳盛
Lui, Truan-Sheng
陳立輝
Chen, Li-Hui
學位類別: 碩士
Master
系所名稱: 工學院 - 材料科學及工程學系
Department of Materials Science and Engineering
論文出版年: 2009
畢業學年度: 97
語文別: 中文
論文頁數: 69
中文關鍵詞: 異質摩擦攪拌銲接鋁合金
外文關鍵詞: aluminum alloy, dissimilar friction stir welded
相關次數: 點閱:150下載:2
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  • 7075鋁合金具有高比強度的特性,屬於高強度型的鋁合金;A356鋁合金擁有良好的鑄造性,經常以鑄造件被使用。在工業零件或運動商品上,常有需要承受較高應力的部位,以及需要以鑄造成型的部位。因此在應用上,7075鋁合金與A356鋁合金之接合有其必要性。本實驗以摩擦攪拌銲接進行兩者之異質接合。分別將7075鋁合金置於Advancing side,A356鋁合金置於Retreating side (簡稱,AS7);和與其相反位置 (簡稱,AS3)。隨後進行異質接合,探討異質材料之彼此相對變形阻抗與攪拌時銲道的流動行為之關係。並且改變進給速率 (0.55 mm/s、0.29 mm/s),進而控制銲道的入熱量。探討入熱量對銲道內微觀組織之影響。
    根據實驗結果顯示,在垂直銲道方向拉伸後發現,AS7-0.55、AS3-0.55與AS3-0.29試料皆破斷在A356的熱影響區,且UTS值皆相近。AS7-0.29因為SZ區產生攪拌填補不良所造成之缺陷,使得強度還有延性下降。
    AS7-0.55、AS3-0.55與AS3-0.29在SZ區皆分為三區 (7075、A356、機械冶金區)。在機械冶金區產生相變化,此相為7075之Mg與A356之Si在摩擦攪拌後所產生,其為大小約為1~2µm之Mg2Si。三組不同參數之SZ區的混合度不同,AS7-0.55最佳,其次為AS3-0.29,最後是AS3-0.55;混合度越佳時,SZ區的機械冶金區越多。在平行銲道方向拉伸時,SZ區的強度及延伸率與機械冶金區之面積呈現正相關趨勢之特性;AS7-0.55的機械性質均優於AS3-0.29;AS3-0.55銲道內產生類似Lazy-S之氧化介在物導致強度偏低。

    7075 alloy is a high strength aluminum alloy, and the A356 alloy has excellent casting property. For the application, combination of 7075 and A356 alloys are necessary. In this study, the friction stir welding is applied for welding 7075 alloy and A356 alloy. In friction stir welding, the flowing behavior and heat quantity will affect the microstructure of welded zone. Furthermore, influences of different microstructures on tensile properties should be considered. Thus, with different welding speed and different welding positions of 7075/A356 specimens, the effects of heat quantity and flowing behavior on microstructures and tensile properties of dissimilar friction stir welded 7075 and A356 are investigated.
    According to the tensile testing which performed along the direction perpendicular to welding direction, the fracture of AS7-0.55, AS3-0.55, and AS3-0.29 are all occurred at the HAZ of A356, and their UTS are similar. The strength and elongation of AS7-0.29 are decreased due to the defects of SZ which resulted from its worse flowing ability.
    The SZ of AS7-0.55, AS3-0.55, and AS3-0.29 specimens can be separated into three parts (7075, A356, and mechanical alloying zone). The phase transformation will be taken place in the mechanical alloying zone. A new second phase of Mg2Si produced when violent friction occurred between 7075 and A356. The mechanical alloying zone of AS7-0.55 is larger than AS3-0.29, and AS3-0.55 displays the least of all. According to the tensile testing which performed along the direction longitudinal to welding direction, the strength and elongation are increased with rising the area of mechanical alloying zone, so the tensile mechanical properties of AS7-0.55 is better than AS3-0.29. The

    existed Lazy-S compound at SZ results in decreasing the tensile strength of the AS3-0.55 specimens.

    總目錄 中文摘要 I 英文摘要 II 總目錄 IV 表目錄 VII 圖目錄 VIII 第一章 前言 1 第二章 文獻回顧 2 2-1 7075鋁合金及A356鋁合金介紹 2 2-1-1 7075鋁合金之析出機制 2 2-1-2 A356鋁合金之析出機制 3 2-1-3 7075鋁合金及A356鋁合金之應用 3 2-2 摩擦攪拌接合之特性 4 2-2-1摩擦攪拌接合原理 4 2-2-2摩擦攪拌接合之流動機制 5 2-2-3入熱量對銲道的影響 6 第三章 實驗方法與步驟 9 3-1 材料製備 9 3-2 摩擦攪拌接合 9 3-2-1 異質接合之試片取樣 9 3-2-2 異質接合製程 10 3-3 微觀組織特性觀察 10 3-3-1 微觀組織觀察 10 3-3-2 微觀組織定性分析 11 3-3-3 微觀組織定量化方式 11 3-4 硬度及拉伸試驗 11 3-4-1 硬度測試 11 3-4-2 拉伸測試 12 第四章 實驗結果 19 4-1 A356與7075 FSP前後之微觀組織與機械性質 19 4-2 接合組織與拉伸及微硬度測試之結果 19 4-2-1 拉伸測試之結果 19 4-2-2不同攪拌參數之銲道形貌 20 4-2-3 PD面之微硬度測試結果 20 4-3 接合後SZ區中各區之探討 21 4-3-1 AS7-0.55 21 4-3-2 AS3-0.55 22 4-3-3 AS3-0.29 22 4-4 SZ區微觀組織之拉伸測試結果 (平行銲道方向拉伸) 23 4-5平行銲道方向拉伸破斷表面與破斷面之結果 23 4-5-1 AS7-0.55及AS3-0.29 23 4-5-2 AS3-0.55 24 第五章 討論 55 5-1 摩擦攪拌參數對銲道的影響 55 5-2 摩擦攪拌對SZ區相改變之探討 56 5-3 摩擦攪拌後之硬度與機械性質的探討 57 5-3-1 摩擦攪拌之熱效應對銲道的影響 57 5-3-2 AS7-0.55與AS3-0.29平行銲道方向拉伸之裂紋傳播機制 57 5-3-3 AS3-0.55平行銲道方向拉伸之裂紋傳播機制 58 第六章 結論 64 參考文獻 65 表目錄 表3-1 7075鋁合金化學組成 (wt.%) 13 表3-2 A356鋁合金化學組成 (wt.%) 13 表4-1 7075-T6母材之平均晶粒徑 25 表4-2 母材及其FSP後之機械性質 26 表5-1 摩擦攪拌異質接合後SZ區中各區之微硬度測試 59 圖目錄 圖2-1 Al-Si 二元相圖 7 圖2-2 ADC12摩擦攪拌進給速率對銲道的影響 8 圖3-1 實驗流程圖 14 圖3-2 (a) 7075-T6材取樣位置;(b) A356-T6材取樣位置 15 圖3-3 FSW示意圖 16 圖3-4 FSW尺寸示意圖 17 圖3-5 (a)拉伸試片取樣圖;(b)拉伸試片尺寸示意圖 18 圖4-1 7075-T6母材的顯微組織 (OM) 27 圖4-2 7075-T6母材之晶出物EDS分析:Al3(Fe,Cr) 28 圖4-3 A356-T6母材之顯微組織 (OM):(a)有鑄造缺陷; (b)無鑄造缺陷。 29 圖4-4 A356-T6母材之晶出物EDS分析:Al9Fe2Si2 30 圖4-5 母材經由FSP後之微觀組織:(a)7075-F;(b)A356-F 31 圖4-6 FSW異質接合後之垂直銲道拉伸機械性質: (a)降伏強度 (YS) 及抗拉強度 (UTS); (b)均勻延伸率 (UE)及總延伸率 (TE) 32 圖4-7 垂直銲道方向拉伸之試片破斷巨觀觀察: (a) AS7-0.55 PD ;(b)AS3-0.55 PD;(c)AS3-0.29 PD;(d) AS7-0.29 PD 33 圖4-8 各參數之PD面微觀組織 (OM): (a)AS7-0.55;(b) AS3-0.55;(c)AS7-0.29;(d) AS3-0.29 34 圖4-9 (a)AS7-0.29 SZ區之缺陷 (OM);(b)缺陷與SZ區的相對位置示意圖 35 圖4-10 摩擦攪拌接合後PD面之微硬度分佈 36 圖4-11 AS7-0.55 FSW後顯微組織 (OM) 37 圖4-12 AS7-0.55 SZ中各區塊之EDS分析:(a)7075區;(b)複合區 ;(c)A356區 38 圖4-13 4-13 EPMA分析AS7-0.55 SZ區中之機械冶金區:(a)複合區;(b)複合層 39 圖4-14 AS7-0.55 SZ區中之復合層:(a)SEM圖;(b)其中之黑色介在物之EDS分析 40 圖4-15 AS3-0.55 FSW後顯微組織 (OM) 41 圖4-16 (a)AS3-0.55流紋狀排列介在物之SEM照片 (下頁續) 42 圖4-16 (b)AS3-0.55流紋介在物EDS分析 (a處) ; (c) AS3-0.55流紋介在物旁基材EDS分析 (b處)。 (續前頁) 43 圖4-16 (d) AS3-0.55流紋狀排列介在物之大倍率SEM照片 (續前頁) . 44 圖4-17 AS3-0.29 FSW後顯微組織 (OM) 45 圖4-18 FSW異質接合後之平行銲道方向拉伸機械性質: (a)降伏強度 (YS) 及抗拉強度 (UTS); (b)均勻延伸率 (UE) 及 總延伸率 (TE) 46 圖4-19 平行銲道方向拉伸 之 試 片 破 斷巨 觀 觀 察 : (a)AS7-0.55; (b)AS3-0.55;(c)AS3-0.29 47 圖4-20 AS7-0.55 平行銲道方向拉伸之破斷次表面 (OM):(a)A356區; (b)複合區 48 圖4-21 AS7-0.55 平行銲道方向拉伸之破斷面 (SEM) :(a)巨觀圖 ; (b)A356區;(c)複合區 (下頁續) 49 圖4-21 (d) AS7-0.55平行銲道方向拉伸之破斷面複合區之 EDS 分析 (續前頁) 50 圖4-22 AS3-0.29 平行銲道方向拉伸之破斷次表面 (OM):(a)A356區;(b)複合區 51 圖4-23 AS3-0.29 平行銲道方向拉伸之破斷面 (SEM): (a) 巨觀圖; (b)A356區;(c)複合區 52 圖4-24 AS3-RS7-0.55 平行銲道方向拉伸之破斷面: (a) 巨觀圖; (b) A356區;(c) 7075區 53 圖4-25 AS3-RS7-0.55 平行銲道方向拉伸之破斷次表面(OM):(a)A356 區;(b)7075區 54 圖5-1 7075-FSP SZ區觀察 (SEM) 60 圖5-2 A356-FSP SZ區觀察 (SEM) 61 圖5-3 SZ區中A356區之微裂紋起始處觀察 (OM): (a)AS7-0.55 ;(b)AS3-0.29 62 圖5-4 微裂紋起始處旁之Si顆粒觀察 (OM):(a)AS7-0.55;(b)AS3-0.29 63

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