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研究生: 陳皇均
Chen, Huang-Jun
論文名稱: 探討疊差能對冷軋黃銅、鎳及銅織構與微結構之影響
Effect of Stacking Fault Energy on Cold-Rolling Texture and Microstructure of Brass, Nickel and Copper
指導教授: 郭瑞昭
Kuo, Jui-Chao
學位類別: 碩士
Master
系所名稱: 工學院 - 材料科學及工程學系
Department of Materials Science and Engineering
論文出版年: 2015
畢業學年度: 103
語文別: 中文
論文頁數: 127
中文關鍵詞: 疊差能黃銅微結構組織織構X光繞射電子背向散射繞射
外文關鍵詞: Stacking fault energy, Microstructure, Texture, XRD, EBSD
相關次數: 點閱:90下載:4
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  • 面心立方金屬變形組織、軋延織構及再結晶織構受疊差能影響甚巨,因此本研究針對面心立方金屬探討疊差能於冷軋延過程中織構演化,實驗材料為多晶鎳、銅、及黃銅,鎳、銅、及黃銅分別代表著高中低三種不同疊差能的面心立方金屬,而壓延量分別為30%、60%和90%。冷軋後以XRD和EBSD分析冷軋織構和顯微組織。
    研究結果為鎳與銅經軋延90%後於β-fiber有著整體強度上升的趨勢晶體方位轉至Copper{112}<111>、S{123}<634>和Brass{110}<112>方位分量,顯示高疊差能材料其冷軋織構為Copper型織構,並於微結構出現層狀次晶粒結構以降低其系統應變能。
    冷軋黃銅中則顯示於軋延30%之後為數多的晶粒因機械雙晶的產生由Copper{112}<111>轉向TC{552}<115>和接近Goss{110}<001>方位,使由Copper型織構轉變為Brass型織構;於冷軋90%時剪切帶出現並由Goss{110}<001>轉向Brass{110}<112>,顯示低疊差能材料冷軋後為Brass型織構,且剪切帶集中區域有著應變能下降之回復現象。

    In this study evolution of texture and microstructure in nickel, copper and brass of fcc metals was investigated. X-ray diffraction and electron backscatter diffraction techniques were used to characterize microstructures and orientation distributions of specimens after 30, 60 and 90% thickness reductions.

    It was found that nickel and copper of high and medium SFE materials show Copper-type texture, and have high orientation densities along the whole β-fiber with increasing deformation. Micro-shear bands are formed when D orientation rotates to Copper and Goss orientation.

    For brass after 30% reduction the orientation of deformed grains changes from Copper {112} <111> to TC{552}<115> close to Goss {110} <001>. Furthermore, the texture type also changes from Copper to Brass type. After 90% cold rolling, shear bands occur in brass and the orientation changes from Goss{110}<001> to Brass{110}<112>.

    摘要 I Extended Abstract II 誌謝 XX 總目錄 XXII 表目錄 XXIV 圖目錄 XXV 第一章 前言 1 第二章 文獻回顧 3 2.1 冷軋微結構與織構 3 2.1.1 FCC金屬與合金其微結構 5 2.1.2 FCC金屬與合金其織構 16 2.2 疊差能於變形結構之影響 23 第三章 實驗流程與分析方法 25 3.1 試片製備 25 3.2 冷軋流程 25 3.3 分析方法 26 3.3.1 X光繞射分析 27 3.3.2 電子背向散射繞射儀 33 第四章 實驗結果 35 4.1 冷軋鎳 35 4.1.1 織構分析 35 4.1.2 微結構分析 47 4.2 冷軋銅 58 4.2.1 織構分析 58 4.2.2 微結構分析 69 4.3 冷軋黃銅 78 4.3.1 織構分析 78 4.3.2 微結構分析 90 第五章 討論 99 5.1 疊差能與FCC織構之關係 99 5.2 疊差能與FCC微結構關係 113 第六章 結論 120 參考文獻 121

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