簡易檢索 / 詳目顯示

研究生: 林彥莛
Lin, Yen-Ting
論文名稱: 具溫度補償之重量量測系統設計製作及其矽膠吸附水汽量測應用
Construction of a Weight Measurement System with Temperature Compensation and its Application to Moisture Adsorption by Silica Gel
指導教授: 楊天祥
Yang, Tian-Shiang
共同指導教授: 陳國聲
Chen, Kuo-Shen
學位類別: 碩士
Master
系所名稱: 工學院 - 機械工程學系
Department of Mechanical Engineering
論文出版年: 2016
畢業學年度: 104
語文別: 中文
論文頁數: 76
中文關鍵詞: 電容式位移感測器熱變形溫度補償溫度延遲重量量測平台
外文關鍵詞: capacitive displacement sensor, thermal deformation, temperature compensation, temperature delay, weight measurement system
相關次數: 點閱:150下載:0
分享至:
查詢本校圖書館目錄 查詢臺灣博碩士論文知識加值系統 勘誤回報
  • 選用適當的多孔性吸附劑,並了解吸附劑的吸附行為,乃為設計一固體式吸附系統的首要課題。而吸附劑的吸附能力表現與吸附劑的密度、吸附劑粒徑大小、吸附劑表面的孔洞大小以及被吸附劑的溫度、壓力與濃度有關。然而矽膠使用不同方法量測時其吸附行為會有一定的差異,故為了定量掌握本實驗室所使用之矽膠的吸附特性,設計一適用之重量量測平台相當重要,也正是本論文研究的首要目標。
    故本研究自行設計一重量量測平台,其中主要實驗方法為使用對位移具有相當高敏感度的電容式位移感測器,來量測矽膠在吸附水汽過程中其自身的重量變化所造成結構上的位移變化,進而得知其重量變化。然而矽膠在吸附過程中將釋放出大量的吸附熱,導致溫度上升,並使得結構因溫度不均勻而產生局部熱變形。這對量測位移變化來轉換成重量變化會有很大的誤差,故必須得知溫度與熱變形之間的關係,並進行溫度補償的動作。
    在實驗中我們分別選擇取樣週期為1min、3min來量測矽膠重量的動態變化。由實驗結果來看,未使用溫度補償來換算重量會與實際吸附水汽量有很大的誤差。而溫度補償則以參考載盤下方溫度當參考溫度,且使用溫度延遲的補償方法可以補償熱變形所帶來的誤差。

    The first step of designing a solid adsorbent moisture adsorption system is choosing an appropriate porous adsorbent and understanding the adsorption behavior of solid adsorbent. The adsorption performance of solid adsorbent is related to the density, size of adsorbent and the size of porous hole on adsorbent surface, also is related to the temperature, pressure and concentration of adsorbate. However, different results of the adsorption performance of adsorbent typically are observed, when different methods are used to measure the adsorption behavior of silica gel. In order to understand adsorption performance of our own silica gel, it is important to design a suitable weight measurement system. And this is the most important goal in this research.
    In this research we design our own weight measurement system. The experiment method is based on the use of a capacitive displacement sensor to design weight measurement system. Capacitive displacement sensor has high sensitivity on displacement change, and therefore is a suitable displacement sensor to measure structure’s small displacement change caused by the weight change of silica gel in adsorption process. However, as silica gel releases large amount of adsorption heats and let the temperature around structure raise, in the adsorption process the temperature of structure starts to be nonuniform and has local thermal deformation inside of structures. As a result, thermal deformation will result in a big experiment error, so we need to know the relation between temperature and thermal deformation and use that to compensate thermal deformation.
    We choose 1min and 3min as sampling time in our experiments, and use these two different sampling times to measure weight change dynamic curve of silica gel in adsorption process. From the experimental results we obtained, it is seen that a large error in the water vapor weight adsorbed by silica gel would arise if we don’t use thermal compensation to calculate adsorption weight from experiment data. We use the temperature under plastic plate as reference temperature when we use thermal compensation to calculate adsorption weight from experiment data. It can compensate thermal deformation error by delaying the time of temperature

    中英文摘要 II 致謝 X 目錄 XII 表目錄 XVI 圖目錄 XVIII 符號說明 XXII 1 緒論 1 1.1 前言 1 1.2 研究動機與目的 4 1.3 文獻回顧 7 1.3.1 等溫吸附曲線 7 1.3.2 固體側擴散係數 11 1.4本文架構 13 2 量測平台設計相關之材料力學公式 15 2.1 結構施力變形 15 2.2 結構熱變形 17 3 重量量測系統設計 21 3.1 重量量測方法介紹 21 3.1.1 電阻應變式 21 3.1.2 電容式 22 3.1.3 電磁式 23 3.2 實驗方法與硬體介紹 24 3.2.1 實驗方法 24 3.2.2 硬體介紹 25 3.3 重量量測系統設計 32 3.3.1 重量量測平台設計 33 3.3.2 造霧系統設計 36 3.3.3 量測介面設計 37 3.4 重量量測平台校正 40 3.4.1 電壓-重量校正曲線 40 3.4.2 溫度補償係數曲線 43 4 實驗架構與流程 47 4.1 實驗系統架構 47 4.2 實驗流程 49 4.3 實驗數據處理 51 5 實驗結果與討論 55 6 結論與未來工作 69 6.1結論 69 6.2本文貢獻 70 6.3未來工作 71 參考文獻 73

    [1] A. Jemni, S. B. Nasrallah, and J. Lamloumi, "Experimental and theoretical study of a metal–hydrogen reactor," International Journal of Hydrogen Energy, vol. 24, pp. 631-644, 1999.

    [2] A. Jemni and S. B. Nasrallah, "Heat and mass transfer models in metal-hydrogen reactor," International Journal of Hydrogen Energy, vol. 22, p. 10, 1997.

    [3] H. Dhaou, F. Askri, M. Bensalah, A. Jemni, S. Bennasrallah, and J. Lamloumi, "Measurement and modelling of kinetics of hydrogen sorption by LaNi5 and two related pseudobinary compounds," International Journal of Hydrogen Energy, vol. 32, pp. 576-587, 2007.

    [4] F. Askri, "Study of two-dimensional and dynamic heat and mass transfer in a metal–hydrogen reactor," International Journal of Hydrogen Energy, vol. 28, pp. 537-557, 2003.

    [5] F. Askri, "Dynamic behavior of metal–hydrogen reactor during hydriding process," International Journal of Hydrogen Energy, vol. 29, pp. 635-647, 2004.

    [6] F. Askri, "Prediction of transient heat and mass transfer in a closed metal–hydrogen reactor," International Journal of Hydrogen Energy, vol. 29, pp. 195-208, 2004.

    [7] A. Jemni and S. B. Nasrallah, "Study of two-dimensional heat and mass transfer during desorption in a metal-hydrogen reactor," International Journal of Hydrogen Energy, vol. 20, p. 10, 1995.

    [8] A. Jemni and S. B. Nasrallah, "Study of two-dimensional heat and mass transfer during desorption in a metal-hydrogen reactor," International Journal of Hydrogen Energy, vol. 20, p. 11, 1995.

    [9] 蔡孟龍,"金屬氫化物儲氫系統之熱流分析:釋氫壓力控制與導熱發泡金屬體積比對系統性能之影響," 博士論文,機械所,國立成功大學,2012
    .
    [10] 朱鼎舜,"釋氫壓力控制對金屬儲氫罐供氫性能的影響,"碩士論文,機械所,國立成功大學, 2008.

    [11] 崔瑋麟,"金屬氫化物顆粒儲氫性能之理論建模與數值模擬,"碩士論文,機械所,國立成功大學, 2010.

    [12] 李承恩,"金屬氫化物儲氫系統中導熱發泡金屬體積比分佈對系統性能之影響,"碩士論文,機械所,國立成功大學, 2011.

    [13] 莊凱茜,"發泡金屬體積比空間分佈對金屬氫化物儲氫系統效能影響之數值分析,"碩士論文,機械所,國立成功大學,2014

    [14] 陶斯塔,"發泡金屬體積比對金屬氫化物儲氫系統週期性儲/釋氫效能影響之數值分析,"碩士論文,機械所,國立成功大學,2014

    [15] 吳健銘,"多孔性吸附反應器熱管理之實驗研究,"碩士論文,機械所,國立成功大學,2012

    [16] 林尚賢,"多孔性吸脫附反應氣熱管理效能之實驗分析,"碩士論文,機械所,國立成功大學,2013

    [17] A. A. Pesaran,"Moisture transport in silica gel Particle Beds,"PHD thesis,School of engineering and Applied Science,UCLA,1983

    [18] C. C. Ni, J. Y. San ,"Measurement of apparent solid side mass diffusivity of a water vapor silica gel system,"International Journal of Heat and Mass Transfer,45 1839-1847,2002

    [19] K.C. Ng, H.T Chua,T. Kashiwagi, B.B. Saha,"Experimental investigation of the silica gel-water adsorption isotherm characteristics," Applied Thermal Engineering, vol. 21, pp. 1631-1642, 2001.

    [20] J.Y. Qiu,"Characterization of silica gel–water vapor adsorption and its measuring facility",Master Thesis,Natonal university of Singpore,2003

    [21] J.E. Ahlberg,"Rates of water vapor adsorption from air by silica gel," Industrial and Engineering Chemistry,1939:31:988-92

    [22] S.S. Hubard, "Equlibrium data for silica gel and water vapor," Industrial and Engineering Chemistry,1954;46:356-58

    [23] S.H. Jury, H.R. Edwards, "The silica gel-water vapor sorption therm," The Canadian Journal of Chemical Engineering,1971;49:663-66

    [24] D.J. Close, P.J. Banks, "Coupled Equlibrium Heat and Single adsorbate Transfer in Fluid Flow through A Porous Medium Prediction for a silica gel air drier using Characteristic Charts," Chemical Engineering Science,1972;27:1157-69

    [25] J.Y. Andersson, H. Bjurstrom, M. Azoulay, B. Carlsson,”Experimental and Theoretical Investigation of the Kinetics of the Sorption of Water Vapour by Silica Gel, ” Journal of the Chemical Society,Faraday.1,1985,81,2681-2692

    [26] L.K. Lee, D.M. Ruthven, "Analysis of thermal effects in adsorption rate measurement," Journal of the Chemical Society,Faraday,1979;75;2406-22

    [27] L.T. Lu, D. Charoensupaya, Z. Lavan, ” Determination of Sorption Rate and Apparent Solid-Side Diffusivity of Pure H2O in Silica Gel Using Constant volume variable pressure appatatus,” Journal of Solar Energy Engineering,1991;113:257-63

    [28] M. Kocirik, P. Struve, M. Bulow, "Analytical sorption of simutaneous mass and heat transfer in zeolite crystals under cinstant volume/variable pressure condition.," Journal of Chemical Society:Faraday Transaction,1984;80:2167-74

    [29] K. Liu, M. J. Sun, T. J. Zhu, Y. L. Wu, Y. Liu, "Modeling and compensation for spindle’s radial thermal drift error in a vertical machining center," International Journal of Machine Tools & manufacture, pp. 58-67,2016.

    [30] R. Li, Y. Zhao, "Dynamics error compensation for industrial robot based in the thermal effect model," International Journal of Measurement, pp. 113-120,2016.

    [31] G. Song, X. Zhou, W. Binienda, "Thermal deformation compensation of a composite beam using piezoelectric actuators," Smart Material And Structures, vol. 13, pp. 30-37,2004.

    [32] 科學online, http://highscope.ch.ntu.edu.tw/wordpress/?p=46860

    [33] 線性熱膨脹係數, https://en.wikipedia.org/wiki/Thermal_expansion

    [34] 應變規原理,麥思科技公司,http://www.memstec.com.tw/product.php?pid=428

    [35] 平行板電容器,
    https://zh.wikipedia.org/wiki/%E7%94%B5%E5%AE%B9%E5%99%A8

    [36] 電磁式電子天平,
    http://bbs.instrument.com.cn/topic/5425652_1?order=threadid

    無法下載圖示 校內:2021-08-23公開
    校外:不公開
    電子論文尚未授權公開,紙本請查館藏目錄
    QR CODE