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研究生: 張群和
Chang, Chin-He
論文名稱: 高溫環境下高鋁水泥之III型斷裂韌度量測與其基本力學性質之研究
A Study of Measuring the Mode III Fracture Toughness and Basic Mechanical Properties of Calcium Aluminate Cement at High Temperatures
指導教授: 王建力
Wang, Chein-Lee
學位類別: 碩士
Master
系所名稱: 工學院 - 資源工程學系
Department of Resources Engineering
論文出版年: 2016
畢業學年度: 104
語文別: 中文
論文頁數: 84
中文關鍵詞: 斷裂力學III型斷裂韌度高鋁水泥
外文關鍵詞: Fracture Mechanics, Mode III fracture toughness, Calcium aluminate cement
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  • 本研究針對含邊緣裂縫之高鋁水泥(Calcium Aluminate Cement)試體,進行反平面剪力試驗以量測III型斷裂韌度。本研究之實驗條件為無圍壓及簡單荷重加載下,進行一套室內III型斷裂試驗程序,設計三種加載方式,分別為90o環狀邊緣加載、70o環狀邊緣加載及裂縫表面加載,探討III型斷裂韌度與其他力學性質之關聯性。
    本研究之高鋁水泥,其Al2O3含量約為40%,以水灰比為0.4拌製純水泥漿,試體分成25℃、200℃、400℃三組溫度歷時,於指定溫度鍛燒24小時,待其降至25℃之後進行試驗,量測其密度、動態泊松比、III型斷裂韌度、單軸壓縮強度、壓入硬度指數、彎矩破壞模數。
    本研究發現:70o環狀邊緣加載為可靠穩定之III型斷裂韌度量測方式,高鋁水泥經過鍛燒之後,其密度、動態泊松比、III型斷裂韌度、單軸壓縮強度、壓入硬度指數、彎矩破壞模數皆有下降之趨勢,III型斷裂韌度的下降情形與彎矩破壞模數較為接近,動態楊氏係數呈現先升後降的趨勢。

    To measure the mode III fracture toughness (KIIIc) of calcium aluminate cement, single edge-cracked Brazilian disks under an anti-plane shear loading condition were proposed in this study. Three loading fixtures: 70o circular loading, 90o circular loading, and crack-edged loading, were arranged and compared in this study. A theoretical formula developed by Chen (2009) were adopted in this study. The disk specimens were prepared and made by calcium aluminate cement. The mode III fracture toughness test was applied by a simplistic load condition. These samples were calcined at 200℃, and 400℃, respectively, and were cooled to room temperature. Then a series of mechanical experiments were conducted on these samples. Correlations between various mechanical properties and mode III fracture toughness were discussed. Results show that experimental values of uniaxial compressive strength, indentation hardness index, modulus of rupture, and mode III fracture toughness decreases while temperature increases. It was observed that the relationships between mode III fracture toughness and modulus of rupture have the best linear correlation than others. The test proposed by Chen is a reliable method for measuring the mode III fracture toughness. The results also demonstrate that 70o circular loading condition achieves the most desirable experimental conditions.

    第一章 緒論 1 1.1 研究背景與動機 1 1.2 研究目的與內容 1 第二章 文獻回顧 4 2.1 研究材料的斷裂力學發展 4 2.2 斷裂韌度之理論發展 6 2.3 III型斷裂韌度相關實驗及模擬 9 2.3.1 邊緣裂縫扭轉試驗 9 2.3.2 懸臂樑撕裂試驗 14 2.3.3 反平面平板彎曲試驗 16 2.3.4 邊緣缺口圓盤彎曲試驗 21 2.3.5 其它III型斷裂韌度試驗 25 2.3.6 III型斷裂韌度試驗之比較 27 2.4 溫度對高鋁水泥性質之影響 29 第三章 研究設備與試驗步驟 35 3.1 試驗規劃 35 3.2 複合楔形體之反平面剪力理論 35 3.3 試驗設備 40 3.3.1 軸向載重系統 40 3.3.2 資料擷取系統 43 3.3.3 Oster材料攪拌機 43 3.3.4 試體製備用機械 44 3.3.5 超音波量測儀 45 3.4 高鋁水泥材料性質 45 3.5 模具介紹及試體製備流程 46 3.5.1 高鋁水泥試體製備流程 47 3.5.2 單軸壓縮試驗之圓柱試體模具 47 3.5.3 III型斷裂試驗之邊緣裂縫圓盤試體模具 47 3.5.4 壓入硬度試驗之製備模具 49 3.5.5 四點彎矩試驗之製備模具 50 3.6 反平面剪力加載模具介紹 51 3.7 試驗方法 54 3.7.1 超音波量測試驗 54 3.7.2 單軸壓縮試驗 55 3.7.3 壓入硬度試驗 56 3.7.4 四點彎矩試驗 57 3.7.5 III型斷裂韌度量測 58 第四章 試驗結果與討論 60 4.1 材料基本物理性質 60 4.2 高鋁水泥高溫後基本力學試驗 62 4.2.1 高鋁水泥高溫後單軸壓縮試驗 63 4.2.2 高鋁水泥高溫後壓入硬度試驗 63 4.2.3 高鋁水泥高溫後四點彎矩試驗 64 4.3 III型斷裂韌度量測 65 4.3.1 試體裂紋擴展觀察 65 4.3.2 90°環狀邊緣加載III型斷裂韌度(KIII) 67 4.3.3 70°環狀邊緣加載III型斷裂韌度(KIII) 67 4.3.4 裂縫表面加載III型斷裂韌度(KIII) 68 4.4 高溫後試體觀察 69 4.5 基本物理及力學性質與III型斷裂韌度之討論 71 4.5.1 不同加壓方式下III型斷裂韌度之討論 71 4.5.2 密度與III型斷裂韌度之討論 73 4.5.3 III型斷裂韌度量測試驗與P波及S波速率之討論 74 4.5.4 III型斷裂韌度量測試驗與單軸壓縮試驗之討論 75 4.5.5 III型斷裂韌度量測試驗與壓入硬度試驗之討論 76 4.5.6 III型斷裂韌度量測試驗與四點彎矩試驗之討論 77 第五章 結論與建議 79 5.1 結論 79 5.2 建議 80 參考文獻 81

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