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研究生: 陳佩宜
Chen, Pei-Yi
論文名稱: 方向性凝固之界面熱傳與溫度場分析
Analysis of Metal-Mold Interfacial Heat transfer and Temperature Field in Directional Solidification
指導教授: 趙隆山
Chao, Long-Sun
學位類別: 碩士
Master
系所名稱: 工學院 - 工程科學系
Department of Engineering Science
論文出版年: 2011
畢業學年度: 99
語文別: 中文
論文頁數: 137
中文關鍵詞: 方向性凝固逆運算法界面熱傳係數
外文關鍵詞: directional solidification, inverse scheme, interfacial heat transfer coefficient
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  • 方向性凝固之鑄件微結構是沿著某一方向固定成長,本研究則希望利用數值分法分析其凝固過程之溫度場的變化情形。於此分析中,鑄件與模具間的界面熱傳性質的不確定問題會影響到分析的結果,所以本文利用Beck逆運算法與實驗溫測數據來計算鑄件與模具間的界面熱傳係數,再使用此界面熱傳係數來進行溫度場的模擬。
    在本研究之實驗中,使用錫鉛(Sn-90wt% Pb)合金針對不同的模具、加熱器溫度、冷激銅盒溫度及載台下降速率來進行方向性凝固,並觀察其凝固的巨觀微觀金相組織、量取冷卻曲線、估算溫度梯度及分析鑄件離開加熱區時間。
    根據實驗溫測數據,以有限差分法與Beck逆運算法求得在鑄件四周沿軸向與徑向之界面熱傳係數,再依此界面熱傳係數,去計算鑄件凝固時的溫度場變化,並與實驗值作比較。從計算與實驗結果作比較,發現到達液相線與共晶溫度的時間是差不多的,同時兩者之冷卻曲線也很接近,因此本研究所建立的方法用來預測界面熱傳係數並估算溫度場是可行的。

    In the directional solidification, the solidified microstructure grows along a fixed direction. The study is to numerically analyze the temperature variation during the solidification process. In the analysis, the uncertainty of the heat transfer condition between the mold and casting will influence the analysis results. Accordingly, in this thesis, the Beck inverse method with the experimentally temperature-measured data is applied to calculate the interfacial heat transfer coefficients and then the coefficients are used to simulate the temperature fields.

    In the research, the Sn-90wt%Pb alloy is used as the testing material. Different mold materials, heater and copper-chill temperatures and the descending speeds of the platform are utilized for the experiments of directional solidification. In the study, the macro- and micro-structures are observed, the cooling curves are measured, the axial temperature gradients are estimated and the departure time of the casting from the heating zone is analyzed.

    Based on the experimentally measured temperatures, the finite difference method and the Beck inverse scheme are employed to predict the interfacial heat transfer coefficients of the casting along the axial and radial directions. With the coefficients, the temperature distributions of the casting are computed during the solidification processes, which are compared with the experimental ones. From the comparison results, it can be found that the computed arrival times of liquidus and eutectic temperatures are very similar to those taken from the experiments. The computed cooling curves are also very close to the ones measured in the experiments. Consequently, it is feasible to use the method set up in the study to predict the interfacial heat transfer coefficients and to calculate the temperature distributions of the casting during the directional solidification processes.

    摘要 ……………………………...………………………………………Ι Abstract… ……………………………………….…………………………………II 致謝…………………………………………...………………………………III 目錄…………………………………………..………………………………IV 表目錄………………………………………..……………………………...…VI 圖目錄…………………………………...………… …………………………VII 第一章 緒論…………..…………………………………………………………1 1-1 研究動機………………………………………………………...……1 1-2 文獻回顧………………………………………………..…………….2第二章 理論基礎………...….........………….…………………………5 2-1 凝固過程………………………………………………………………….5 2-1-1成核( Nucleation )…………………………………………………..5 2-1-2晶粒成長與侵犯階段( Growth and Impingement )...…………….7 2-1-3晶粒成長型態……………….……………………………………….7 2-2方向性凝固模式………………………………………………………….8 第三章 實驗設備與方法……....…………………….…………..……10 3-1實驗步驟…………..…………….………………………...…….10 3-2實驗參數…….…………………………………………………………...11 3-3實驗設備…………………………………………………………………12 3-3-1 熱電偶點焊與氫氧焰氣焊設備……………………………….…12 3-3-2 溶解爐………………………………………………………….12 3-3-3 方向性凝固載台與冷激端設備…………………………….12 3-3-4 加熱及溫度控制設備……………………….…………………13 3-3-5 溫度擷取設備...……………………………………………….14 3-3-6恆溫循環水槽…………………………………………………….15 3-3-7 方向性凝固之實驗設計………………………………………15 3-4金相顯顯組織的觀察……………………………………………………16 3-5實驗數據整理與計算……………………………………………………18 第四章 數值分析……………..………………………………………………21 4-1 凝固之熱傳模式………………………………………………………...21 4-2 界面熱傳係數之分析..………………………………………………....22 4-3 差分方程式………………………...……………………………………23 4-4 Beck 逆運算法.............................25 4-4-1 Beck 逆運算法的直接問題……………………………………25 4-4-2 Beck 逆運算法的處理模式…………………………………..27 4-5潛熱釋放之計算方法………………………........29 第五章 結果與討論……...……………………………………………………32 5-1 鑄件的巨觀觀察…………………………………………………………32 5-2 鑄件的微觀觀察……………………………………………………….34 5-2-1 橫截面晶粒數及微觀觀察………………………………………34 5-3 界面熱傳係數……..………………………………………………….35 5-3-1 軸向界面熱傳係數………………………………………………36 5-3-2 徑向界面熱傳係數……………………………………………..38 5-4 鑄件的溫度量測與數值比較………………………………………….40 5-5 鑄件的溫度梯度與數值比較………………………………………….41 5-6 鑄件各位置離開加熱區時間和凝固時間的實驗與數值比較.……….42 第六章 結論……………………………………………………………………….44 參考文獻………………………………………………………………………...47 附錄A 晶粒數之取樣方式................................122 附錄B 溫度場之差分方程式推導............124 附錄C 錫鉛合金之潛熱式推導………..……………..…………………135

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