本研究旨在利用煉鋼副產物之高爐集塵灰，經處理後可獲得高純度碳含量之凝析石墨（kish graphite，KG），以電化學插層法將凝析石墨製得石墨插層化合物（graphite intercalation compound，GIC）， 再藉由微波處理製備膨脹石墨（expanded graphite，EG），後續使用2 種市面常見柴油進行吸附試驗，測試膨脹石墨的吸附效能為符合資源再利用之理念，亦進行EG循環性試驗，並評估其循環再利用之能力。
首先，透過粒徑分析了解石墨的粒徑分佈以及元素分析（element analysis，EA）測得凝析石墨之碳含量。接著於電化學插層實驗中設計一組電化學反應裝置進行，以不鏽鋼片作為反應電極，設置一端陽極、另外二端作為陰極，使用硫酸作為插層溶液，以電能取代氧化劑的功用來進行電化學插層反應，探討不同插層反應條件對膨脹體積之影響。最後歸納出凝析石墨在水洗量2000 mL、電流密度240 mA/cm2、硫酸濃度60 %、氧化插層時間15 min、微波功率700 W、微波時間20 s之實驗條件下，可獲得較佳膨脹體積185 mL/g。另外，分別針對304、316型號不鏽鋼電極進行電化學插層重複試驗，以評估在更換與不更換插層溶液之情形下，不同電極對膨脹體積、電極損失量及金屬離子累積釋出量之影響。由結果歸納出在更換溶液下，使用 316 不鏽鋼電極在膨脹體積、電極重量損失及金屬離子損失量的表現較佳，經10次電化學插層反應後仍維持在膨脹體積112 mL/g。
在膨脹石墨吸附油品之試驗中，於超級柴油與甲種漁船燃料油環境下進行吸附，歸納出在吸附溫度30℃、吸附時間10 min的條件下，凝析石墨所製備之膨脹石墨吸附量分別為59.66與64.48 g/g，且皆已達到吸附平衡之97.5%以上。後續應用於脫附試驗中，以脫附溫度300℃、脫附時間15 min 可達到脫附率99.3%。於循環次數之試驗中，經5次吸脫附後，再生率仍維持於55%以上，顯示其具有可循環再利用之能力。
綜合以上結果，由煉鋼集塵灰中所獲得之凝析石墨，可製備為膨脹石墨並應用於油污處理問題，成為一種具有替代天然石墨潛力之吸附材料，符合當前所提倡的資源再生利用和永續循環之理念。

In this study, the kish graphite(KG) from blast furnace dust, a byproduct of steelmaking, was used to prepare graphite intercalation compound (GIC) via an electrochemical intercalation method, and expanded graphite (EG) was prepared by microwave irradiation. The adsorption test of EG was conducted by using two commonly available diesel types. Moreover, to align with the principles of resource reuse, the cyclic test was performed to assess its reusability and recycling potential. With the electrochemical intercalation experiment, a three-electrode system was constructed with stainless steel electrodes, which included an anode in the middle, two cathodes at both ends, and sulfuric acid was used as the intercalation solution. The largest expanded volume is 185 mL/g which was prepared under the parameters of water consumption = 2000 mL, current density = 240 mA/cm2, sulfuric acid concentration = 60 wt%, reaction time = 15 min, irradiation power = 700 W, irradiation time = 20 s. On the other hand, the repeated experiment indicated that with the replacement of the intercalation solution, the expanded volume remained stable at 112 mL/g with Type 316 stainless steel electrode, and its performance was better than Type 304. After adsorption, desorption, and cyclic tests, kish-expanded graphite(EG-K) achieved the maximum adsorption capacity of 64.48 g/g, a desorption rate of 99.3 % at 300℃ for 15 min, and the regeneration rate of EG-K remained above 55% after five cycles, which proved that EG-K is an adsorbent material with the potential for reuse.

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