成功大學博碩士論文系統

簡易檢索 / 詳目顯示

回結果列表

研究生：	林正偉 Lin, Zheng-Wei
論文名稱：	光纖式與全場表面電漿共振之相位量測 Phase Measurement in Fiber-Type and Full-Field Surface Plasmon Resonance
指導教授：	羅裕龍 Lo, Yu-Lung
學位類別：	碩士 Master
系所名稱：	工學院 - 機械工程學系 Department of Mechanical Engineering
論文出版年：	2005
畢業學年度：	93
語文別：	英文
論文頁數：	78
中文關鍵詞：	表面電漿共振、共路徑外差干涉術、D型光纖、全場量測
外文關鍵詞：	full-field measurements, D-shaped fiber, common-path heterodyne interferometer, surface plasmon resonance (SPR)
相關次數：	點閱：91 下載：5
分享至:	分享至facebook 分享至twitter

查詢本校圖書館目錄查詢臺灣博碩士論文知識加值系統勘誤回報

　　本文主要分為兩個部份作為方向，分別是全場表面電漿振量測與D型光纖表面電漿共振感測器。所採用之實驗架構為共路徑外差干涉術。第一部份，利用電荷藕合元件(CCD) 影像截取設備來補取影像，再利用三步還原術重建相位以得所求。第二部份，設計D型光纖面電漿共振感測器來作為光學折射計與應變感測器。前者利用外界折射率的改變以求得，P波和S波的相位差；後者利用改變光纖核部(core)之折射率以得到相位差，此法相對傳統面表電漿共振感測器為一個較新的概念。

　In this thesis, there are two parts we studied: Full-Field Surface Plasmon Resonance (SPR) measurement and optical D-shaped fiber SPR sensor. All the configurations are based on the common-path heterodyne interferometry, and the SPR sensor design based on measuring the differential phase between the s and p polarizations has been demonstrated. In first part, we use CCD (Charged Coupled Device) camera to capture the image, and use the integrated-bucked method to reconstruct the phase term. In second part, we design D-shaped fiber SPR as an optical refractometer and a strain sensor. The former is using the change of the refractive index of the analyte to obtain the phase difference as an optical refractometer, and the latter takes use of altering the refractive index of fiber core to obtain the phase difference as a strain sensor.

Abstract	I
中文摘要	II
Acknowledgment	III
Table of Contents	IV
Table List	VII
Figure List	VIII
Chapter 1 Introduction	1
1.1 Preface	1
1.2 Research Destinations and Motivations	1
1.3 Overview of Chapters	2
Chapter 2 History Review	3
2.1 Overview in the Development of SPR	3
2.2 History Review of Full-Field SPR Measurement	5
2.3 History Review of Fiber SPR Sensors	6
Chapter 3 Fundamental Theory Analysis	10
3.1 Evanescent wave	10
3.1.1 The deriving of Evanescent Wave	10
3. 2 Three-Layer Optical Waveguide Theory	12
3.2.1 Dispersion Relation	12
3.2.2 Attenuator Total Reflector	14
3.2.3 Fresnel Equations	14
3.2.4 Film Thickness [LaFemina, 1995]	16
3.2.5 Simulation Sample – Air and Water	20
3.3 Four-Layer Optical Waveguide Theory	21
Chapter 4 Bulk SPR Sensor	29
4.1 Preface	29
4.2 Common-Path Heterodyne Interferometry	29
4.3 Single-Point Method	29
4.3.1 Intensity-modulation	29
4.3.1.1 Experimental Setup	30
4.3.1.2 Experimental Result	31
4.3.2 Phase modulation	32
4.3.2.1 Experimental Setup	32
4.3.2.2 Result and Discussion	34
4.4 Full-Field Measurements	35
4.4.1 Experimental Setup	35
4.4.2 Integrating-Bucket Method	35
4.4.3 Result and Discussion	37
Chapter 5 Optical D-shaped fiber SPR sensor	48
5.1 Fabrication of the D-shaped Fiber SPR Sensor	48
5.1.1 Etching Rate Measurement	48
5.1.2 Fabrication	49
5.2 Optical D-shaped fiber SPR refractometer	51
5.2.1 Experimental Setup	51
5.2.2 Experimental Result	53
5.2.3 Error Discussion	53
5.3 Optical fiber SPR strain sensor	55
5.3.1 The Variance of the Core in the D-shaped fiber	55
5.3.2 Experiment and Discussion	57
Chapter 6 Future Work	72
6.1 Conclusion	72
6.2 Future Work	72
Bibliography	73
Autobiography	78

Table 4. 1  The sensitivity and the corresponding resolution for single-point method	47
Table 4. 2  The sensitivity and the corresponding resolution for Full-Field measurement	47
Table 5. 1  Etching depth measurement.	70
Table 5. 2  The sensitivity of fiber-type SPR sensor	71

Figure 2. 1  Most widely used configurations of SPR sensors	8
Figure 2. 2  The Kretschmann (a) and Otto (b) configuration.	8
Figure 2. 3  Sinusoidal phase modulating interferometer	9
Figure 3. 1  Snell’s Law and evanescent wave	23
Figure 3. 2  Goos Haenchen Shift	23
Figure 3. 3  The figure of the wave vector	24
Figure 3. 4  ATR coupler	24
Figure 3. 5  Dispersion-Relation (DR)	25
Figure 3. 6  Three layer film theory	25
Figure 3. 7  General medium index of light propagation.	26
Figure 3. 8  The resonance angle and critical angle of Air.	26
Figure 3. 9  The resonance angle of a bulk SPR for pure water.	27
Figure 3. 10  The simulation of phase difference between P-wave and S-wave for pure water.	27
Figure 3. 11  The resonance angle of a fiber SPR for glycerol.	28
Figure 4. 1  The first experiment for intensity-modulation.	39
Figure 4. 2  The diagram of Intensity v.s. incident angle.	39
Figure 4. 3  The diagram of Intensity v.s. refractive index	40
Figure 4. 4  The simulation of Intensity variation for different refractive index.	40
Figure 4. 5  The stability of the intensity-modulation method in a bulk SPR.	41
Figure 4. 6  The experiment setup of single-point SPR measurement.	41
Figure 4. 7  The comparison of single-point method and theoretical analysis.	42
Figure 4. 8  The stability of Single-Point Methd	42
Figure 4. 9  Experimental setup for the full-field measurement.	43
Figure 4. 10  The function of a CCD for general sinusoidal curve.	43
Figure 4. 11  The photo captured by CCD for 0ml and 1ml.	44
Figure 4. 12  The result of full-field measurement.	45
Figure 4. 13 The full plane phase difference between P-wave and S-wave.	45
Figure 4. 14  The stability of the full-field measurement.	46
Figure 5. 1  The etching rate for different material	59
Figure 5. 2  The fabrication flow of the D-shaped optical fiber SPR sensor	60
Figure 5. 3  D-Shaped optical fiber without well stripping plastic coating off.	61
Figure 5. 4  D-Shaped optical fiber with well stripping coating off.	61
Figure 5. 5  The BOE Etching of D-shaped optical fiber	62
Figure 5. 6  DI water and nitrogen cleaning after etching D-shaped fiber by BOE.	62
Figure 5. 7  Experimental setup for a fiber-type SPR sensor.	63
Figure 5. 8  The configuration of D-shaped fiber and its principal axes	63
Figure 5. 9  Illustration of SPR-polarizer	64
Figure 5. 10  Illustration of matching the principal axes between light and D-shaped fiber.	64
Figure 5. 11  Phase difference of fiber-type SPR sensor between P-wave and S-wave relative to variation of nanalyte.	65
Figure 5. 12  The result of fiber-type SPR sensor.	65
Figure 5. 13  The relationship for number of reflection and the incident angle.	66
Figure 5. 14  Phase difference diagram with different incident angle.	66
Figure 5. 15  Phase difference of fiber-type SPR sensor between P-wave and S-wave relative to variation of ncore.	67
Figure 5. 16  The simulation of a general polarimetric fiber strain sensor coated with metal film.	67
Figure 5. 17  The experiment setup for a fiber-SPR strain gauge	68
Figure 5. 18  The result of the fiber-SPR strain gauge sensor	68
Figure 5. 19  The experiment of a general polariemtric fiber strain sensor.	69


                                    

Ashwell, G.J. and Roberts, M.P.S., “Highly selective surface plasmon resonance sensor for NO2”, Electronics Letters, Vol. 32, No. 22, pp. 2089-2091, 1996.

Bertholds, A. and Dandliker, R., “Determination of the individual strain-optic coefficients in single-mode optical fiber”, Journal of lightwave technology, Vol. 6, No. 1, 1998.

Chien F.-C., Chenb S.-J., “A sensitivity comparison of optical biosensors based on four different surface plasmon resonance modes”, Biosensors and Bioelectronics, Vol. 20, pp. 633–642, 2004.

Chinowsky, T. M., Quinn, J. G., Bartholomew D. U., “Performance of the Spreeta 2000 integrated surface plasmon resonance affinity sensor”, Sensors and Actuators B, Vol. 91, pp. 266-274, 2003.

Drez, A., Andres, M.V., and Cruz J.L., “In-line fiber-optic sensors based on the excitation of surface plasma modes in metal-coated tapered fibers”, Sensors and Actuators B, Vol. 73, pp. 95-99, 2001.

Eduardo, F., Hector, D. D., Member, IEEE, “Surface plasmon resonance on a single mode optical fiber”, IEEE Transactions on Instrumentation and Measurement , Vol. 47, No. 1, pp. 168-173, 1998.

Grigorenko, A.N., Beloglazov, A.A., Nikitin, P.I., Kuhne, C., Steiner, G., and Salzer, R., “Dark-field surface plasmon resonance microscopy”, Optics Communications, Vol. 174, pp.51–155, 2000.

Homola, J. and Slavik, R., “Fibre-optic sensor based on surface plasmon resonance”, ELECTRONICS LETTERS, Vol. 32 No. 5, pp480-482, 1996.

Jihua, G., Zhaoming, Z., and Weimin, D., “Small-angle measurement based on surface-plasmon resonance and the use of magneto-optical modulation”, Applied Optics, Vol. 38, No. 31, pp. 6550-6555, 1999.

Jiri, H., “Optical fiber sensor based on surface plasmon excitation”, Sensors and Actuators B, Vol. 29, pp. 401-405, 1995.

Jiri, H., Sinclair, S. Yee, and Gunter, G., “Surface plasmon resonance sensors: review”, Sensors and Actuators B, Vol. 54, pp. 3-15, 1999.

Jorgenson, R.C. and Yee, S.S., “A fiber-optic chemical sensor based on surface plasmon resonance,” Sensors and Actuators B, Vol. 12, pp. 213–220, 1993.

Kano, H. and Kawata, S., “Surface-plasmon sensor for absorption-sensitivity enhancement”, Applied Optics, Vol. 33, No. 22, pp. 5166-5170, 1994.

Kao, C. K., Optical Fibre, IEE MATERIALS & DEVICES SERIES, pp. 96-99, 1988.

LaFemina, J. P., Chemistry and Physics of Surfaces and Interfaces, CRC Series, pp133-140, 1995.

Lee, B., “Review of the present status of optical fiber sensors”, Optical Fiber Technology, Vol. 9, pp. 57–79, 2003.

Markos, D. J., Ipson, B. L., Smith, K. H., Schultz, S. M., Selfridge, R. H., Monte, T. D., Dyott, R. B., and Miller G., “Controlled core removal from a D-shaped optical fiber”, Applied Optics, Vol. 42, No. 36, 2003.

Muhammad, F. A., Raweshidy, H. S., and Senior, J. M., “Polarimetric optical D-fiber sensor for chemical application”, Microwave and Optical Technology Letters, Vol. 19, No. 5, pp. 318-321, 1998.

Palumboa, M., Pearsona, C., Nagelb, J., and Petty M.C., “A single chip multi-channel surface plasmon resonance imaging system”, Sensors and Actuators B, Vol. 90, pp. 264–270, 2003.

Raether, H., Surface plasmons on smooth and rough surfaces and on gratings, Springer-Verlag, Berlin, 1988.

Regis, J. V. and George, S. S., Strain and Temperature Measurement with Fiber Optic Sensors, Technomic Pub. Co., Lancaster, Pa., pp. 6 & pp. 276-277, 1997.

Sasaki, O., Okazaki, H., and Sakai, M., “Sinusoidal phase modulating interferometer using the integrating-bucket method”, Applied Optics, Vol. 26, No. 6, pp.1089-1093, 1987.

Senior, J. M., Optical Fiber Communications, Principles and Pratice, 1985.

Shuai, S., Tong, L., and Jihua, G., “Optical phase-shift detection of surface plasmon resonance”, Applied Optics, Vol. 37, No. 10, pp. 1747-1751, 1998.

Su, Y.-D., Chen S.-J., and Yeh, T.-L., “Common-path phase-shift interferometry surface plasmon resonance imaging system”, Optics Letters, Vol. 30, No. 12, pp. 1488-1490, 2005.

UDD, Eric, Fiber Optic Smart Structures, Wiley, New York, pp179-185, 1995.

Ward, L., The Optical constants of bulk materials and films, Institute of Physics Pub., Bristol, pp. 166-171, 1994.

Yu, X., Wang, D., Wang, D., Ou, Y. J. H., Yan, Z., Dong, Y, Liao, W., and Zhao, X. S., “Micro-array detection system for gene expression products based onsurface plasmon resonance imaging”, Sensors and Actuators B, Vol. 91, pp. 133–137, 2003.

彭祈程, “D型光纖於表面電漿共振感測器與偏光器之設計與製作”, 國立成功大學機械系, Tainan, Taiwan, R.O.C., June 2004.

池弘偉, “全場式光學外差干涉儀應用於量測雙折射晶體光學參數之設計與研究”, 國立成功大學機械系,Tainan, Taiwan, R.O.C., June 2005.

校內：2008-07-15公開
校外：2008-07-15公開

簡易檢索 / 詳目顯示

相關論文