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研究生: 王世昌
Wang, Shih-Chang
論文名稱: 熱均壓製程對鑄造超合金Inconel 713 LC 顯微組織與機械性質影響之研究
Effect of microstructure and mechanical properties of hot isostatically pressed superalloy Inconel 713 LC
指導教授: 李世欽
Lee, Shi-Chi
學位類別: 碩士
Master
系所名稱: 工學院 - 材料科學及工程學系
Department of Materials Science and Engineering
論文出版年: 2006
畢業學年度: 94
語文別: 中文
論文頁數: 87
中文關鍵詞: 伸長率抗拉強度偏析孔隙率γ'γInconel 713 LC超合金熱均壓
外文關鍵詞: Hot Isostatic Pressing, γ', Inconel 713 LC superalloy, γ, porosity, segregated structure, elongation, tensile strength
相關次數: 點閱:203下載:3
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  • 熱均壓(Hot Isostatic Pressing, HIP)技術已廣泛應用於鑄造工業以去除鑄造過程中所產生之內部孔隙,它結合了高溫及高壓方式以提供材料較佳的性質,並改善鑄造材料的強度、延展性與疲勞壽命。Inconel 713 LC為使用在航太工業上最多的超合金材料,同時具有優越的高溫抗腐蝕性、強度、潛變及疲勞等性質。Inconel 713 LC超合金是典型的γ´ (Ni3Al,Ni3Ti)在γ基地上析出,隨著γ´析出量的增加而提高強度。
    本研究主要探討熱均壓製程對Inconel 713 LC鑄造超合金之影響,Inconel 713 LC超合金實驗中,使用三種不同之熱均壓溫度包括1180、1195與1210 °C;二種不同之熱均壓壓力為1500及1750 Bar;二種不同的保溫保壓時間為2及4小時。同樣利用常溫及高溫拉伸試驗、孔隙率、TEM與XRD顯微結構等分析來評估熱均壓製程對鑄造超合金性質之影響。
    由本研究結果,Inconel 713 LC鑄造超合金的最佳熱均壓製程為1180°C, 1750Bar, 2hours,明顯地降低其孔隙率與增加拉伸強度與伸長率、改善偏析組織。

    Hot Isostatic Pressing (HIP) is widely used in the casting industry to remove the internal porosity generated during the casting process. It combines higher pressure and temperature to produce materials and parts with substantially better properties than those by other methods. This results in improved strength, ductility and fatigue life of castings. Inconel 713 LC is the most widely used superalloy for aerospace applications. The Inconel 713 LC nickel-based superalloy have decent corrosion resistance, high strength and ambient temperature and excellent creep and fatigue strengths at high temperature. Inconel 713 LC superalloy typically consists of γ´ (Ni3Al,Ni3Ti) dispersed in a γ matrix and the strength increases with increasing volume fraction of γ´.
    The aim of this paper is to discuss the methods and to find a suitable soaking time of HIP for Inconel 713 LC superalloy castings. In the study of Inconel 713 LC superalloy, the parameters of HIP process included of three different temperatures are used: 1180, 1195 and 1210°C, two different pressures are used: 1500 and 1750 Bar and two different soaking times are 2 and 4 hours. The Inconel 713 LC superalloy is used throughout this study. To evaluate the mechanical properties and compare the effects of microstructure with tensile properties of Inconel 713 LC superalloy made by HIP process, two different strain rates of tension test at room and high temperature were evaluated. The TEM microstructure and XRD inspections were performed.
    The experiment as results show that 1180°C, 1750 Bar, 2 hours of HIP treatment for Inconel 713 LC superalloy was optimum. It can improve the microstructure and tensile properties of Inconel 713 superalloy castings. Through the optimum HIP treatment the segregated structure is improved.

    中文摘要 I 英文摘要 II 總目錄 IV 圖目錄 VII 表目錄 XI 第一章 前言 1 第二章 文獻回顧 3 2-1 超合金組成元素及作用 3 2-2 合金組織及影響 8 2-3 合金強化機構及理論 9 2-3-1 γ析出硬化 10 2-3-2 基地固溶強化 10 2-3-3 晶界析出強化 10 2-4 熱均壓技術(Hot Isostatic Processing) 11 2-4-1 熱均壓原理 12 2-4-2 熱均壓去除孔隙過程 13 2-4-3 熱均壓設備的構造 14 2-4-4 熱均壓過程 19 2-5 影響Inconel 713 LC機械性質的可能因素 20 第三章 實驗步驟 22 3-1 試片準備 25 3-2熱均壓處理(Hot Isostatic Pressing,HIP) 25 3-3固溶及時效熱處理 31 3-4超合金組織及結構分析 33 3-5密度與孔隙分佈 34 3-6機械性能測試 35 3-6-1硬度測試 35 3-6-2拉伸性能測試 35 第四章 結果與討論 37 4-1成分分析 37 4-2熱差分析 37 4-3 X-RAY分析 39 4-4 顯微組織觀察 39 4-4-1 EPMA分析 43 4-4-2 γ顯微組織分析 53 4-4-3 TEM分析 58 4-4-4 孔隙分佈與密度 67 4-4-5 硬度試驗 69 4-4-6 拉伸試驗 69 4-5破斷面觀察 75 第五章 結論 81 參考文獻 83 誌謝 87

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