等原子鐵鈀合金因其具有較佳的延展性以及在c軸的高磁晶異向性，因而被視為潛力的磁紀錄和高溫磁性應用之材料。由於鐵鈀的c軸優選方位之控制在磁性應用非常重要。因此，本論文將以電鍍與熱機製程方法製備方向性鐵鈀合金。由實驗的結果顯示，電鍍鐵鈀薄膜在500°C、600°C和700°C下退火1小時分別具有<101>，<111>和<421>方向。矯頑磁力隨著退火溫度增加而減少，而平均晶粒尺寸隨著溫度增加而增加。
此論文首先提出相關係數(correlation coefficient)來定量織構量測的相似度。實驗結果與X光繞射(X-ray diffraction, XRD)比較後顯示電子背向散射繞射(electron backscatter diffraction, EBSD)的掃描間距範圍介於1−20 µm之間時，相關係數的數值在冷軋50%以及88%後的試片上趨近於1。結果顯示可以利用20 µm掃描間距在較短的時間內測量織構。
對於熱機製程，冷軋50%的鐵鈀合金其微觀結構主要顯示雙晶層帶以及細雙晶，變形織構為Twin Copper{552}<115>和Copper{112}<111>方位。此外，當冷軋變形量增加至90%時，觀察到的顯微組織則是以細次晶粒與剪切帶為主，並且顯示Goss{011}<100>和Brass{011}<112>等冷軋織構，並且Copper織構的強度隨著變形程度增加而減少。
在序化溫度為530°C下退火後，冷軋50%以及90%厚度減少的鐵鈀合金完全再結晶分別發生在退火時間為400小時和16小時。冷軋50%的試片從Copper織構轉變成為(010)[1101]為主的優選方位，而90%厚度減少的試片經過完全再結晶之後其再結晶織構則是主要為(054)[22-45]方位，並且保留Goss和Brass變形織構。在退火時間為16小時，冷軋50%以及90%的試片可得到最大矯頑磁力分別為932 Oe和519 Oe，而平均晶粒大小分別為2.54 μm和1.57 μm。
實驗結果顯示在無序化溫度為700°C下退火後，冷軋50%的鐵鈀合金完全再結晶發生在退火時間為48小時，並且具有(-1294)[401]和(558)[-1-1510] 方位。而冷軋90%的試片完全再結晶發生在退火時間為1分鐘，其再結晶織構為(6115)[2-713]方位。

FePd alloy has been considered as applications of potential magnetic recording and high temperature magnetic materials, due to exhibiting the high magneto-crystalline anisotropy and good ductile property. Thus, controlling preferential orientation of the c-axis is very importance in magnetic applications. In this thesis; as a result, employs electrodeposition and thermo-mechanical process to induce the preferential orientation in FePd alloy. Experimental results show that electrodeposited FePd films have <101>, <111> and <421> directions after annealing 500°C, 600°C and 700°C for 1 hr, respectively. The value of coercivity (Hc) is decreased with increasing temperatures, whereas the average grain size is increased.
This thesis firstly proposes the concept of the correlation coefficient to quantify the similarity of texture. In comparison with X-ray diffraction (XRD), the experimental results of electron backscatter diffraction (EBSD) show that the correlation coefficient is close to 1 after 50% and 88% cold rolling in the step size range of 1 µm–20 μm. The results show that it can measure texture using a large scanning step of 20 μm at short time.
For thermo-mechanical process, microstructures of cold-rolled 50% FePd alloy mainly exhibit twin lamella band and fine twin structures, deformation textures are the Twin Copper {552}<115> and Copper {112}<111>. Additionally, the microstructures consisting of fine subgrains and shear bands are observed in the sample of 90% deformation which has the rolling textures of Goss {011}<100> and Brass {011}<112> orientations. The intensity of Copper texture is decreased as increasing cold rolling degrees.
During annealing at ordering temperature 530oC, full recrystallization occurs in 50% and 90% cold-rolled FePd alloy for 400 hr and 16 hr, respectively. Dominant texture in cold-rolled 50% sample changes from Copper type to (010)[1101] preferred orientation. Recrystallization texture (054)[22-45] is observed in sample of 90% thickness reduction after full recrystallization, and deformation textures of Goss and Brass are maintained. After 16 hr annealing, the maximum Hc exhibits 932 Oe with average grain size (1.57 μm) for 90% cold-rolled sample, which is 519 Oe with average grain size (2.54 μm) for 50% cold-rolled specimen, respectively.
After 700oC annealing at disordering temperature, fully recrystallization of 50% cold-rolled FePd alloy take place for 48 hr, and recrystallized textures exhibit (-1294)[401] and (558)[-1-1510] orientations. In the case of 90% cold-rolled sample, completely recrystallization occurs after 1 min annealing, and the recrystallized texture is (6115)[2-713] orientation.

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