鐘擺型黏彈頻譜儀(PVS)為一種在不同溫度下，藉由頻率掃描，測量固體黏彈性質的儀器，鐘擺型液體黏彈頻譜儀(LPVS)是用以測量液體黏彈性質之儀器。兩者實驗方式皆以線圈與磁鐵的磁交互作用，使一懸臂樑轉子產生週期性振動，再以雷射位移量測系統精準紀錄其位轉子之變形量，因此可獲得不同頻率下的應力與應變關係。磁交互作用是來自於永久磁鐵及荷姆赫茲線圈所產生的磁場，因此可實現在高頻率下，對試體產生扭矩及純彎矩的加載。對於鐘擺型黏彈頻譜儀，懸臂樑轉子為細長的待測試體。為了防止相對柔軟的物體在測量期間挫曲或其他重力場的影響，PVS試體以鐘擺方式振動，但LPVS轉子以逆鐘擺方式振動。鐘擺型液體黏彈頻譜儀的懸臂樑轉子為一個材料性質已知的固體，藉由轉子與周圍液體環境的交互作用，測量液體的流變性質，以及奈米顆粒懸浮液裡的顆粒大小。本論文探討在LPVS機台建立加熱裝置，測量高溫下試體的流變性質，也提出新轉子的設計，以期未來可用於不同的應用之中。此外，本論文亦對不同的材料系統進行探討，以PVS測量並分析(1)瓦楞紙不同軸向的性質，(2)輪胎橡膠固體的黏彈性質，(3)硬化後水泥漿的時依性質。在100Hz時，瓦楞紙橫向動態楊氏模數jE j =600 MPa，機器向jE j =210 MPa，剪力模數jG j分別為100，50MPa，在扭力與純彎曲變形下，瓦楞紙的正切消散模數各別約為0.042和0.048。本論文亦以LPVS測量並分析(1)凝膠在升溫下的流變性質，(2)奈米顆粒於懸浮液中的粒徑分析。另外，本論文使用LPVS和PVS量測與分析保麗龍膠其液態與固態的黏彈性質之變化，在液態時，其正切消散模數在0.01Hz約為1000，在100Hz約為1，固化後的保麗龍膠其正切消散模數在0.01至100Hz間約為0.5至0.05。此外。本論文亦提出一個機器深度學習的方法，分析懸浮液中的奈米顆粒粒徑以及其分散狀態。

Pendulum-type viscoelastic spectroscopy (PVS) and liquid pendulum-type viscoelastic spectroscopy(LPVS) are developed to measure the viscoelasticity of solids and fluids, respectively,in a frequency sweep at various temperatures. Both experimental methods utilize magnetic interactionto general mechanical vibrations of a cantilever beam, and its deformation is recordedthrough a laser-based displacement measurement system. The magnetic interaction between apermanent magnet and Helmholtz coil can achieve high-frequency driving torque or pure bending moment. For PVS, the cantilever beam is the specimen under testing. For LPVS, the cantilever beam is made of a known material, and interactions between the beam and its surrounding liquid give rise to its rheological properties. In addition to rheological properties, LPVS is also capable of determining the size of nanoparticles in colloidal suspension. Experiments at elevated temperature for LPVS were achieved by wrapping a heating tape around the container that holds the liquid sample. In this work, several new designs of LPVS core components were attempted, and their performances were analyzed. In addition, several samples were studied. Fresh and hardened cement paste were experimentally studied by LPVS and PVS, respectively. A class of glue at its liquid state and hardened state was also investigated. Furthermore, PVS was adopted to study the viscoelastic properties of corrugated cardboard and tire rubber. For the corrugated cardboard, it was obtained that, at 100 Hz, dynamic Young’s modulus jE_j = 600 MPa in cross direction, and jE_j = 210 MPa in machine direction. And dynamic shear modulus jG_j are 100 and 50 MPa. Furthermore, the cardboard showed tan _ about 0.048 in bending mode and 0.042 in torsion mode. For the tire rubber, its damping was measured about 0.1 around 100 Hz. LPVS was utilized to study the rheological properties of nanoparticle colloidal suspensions, glue and a kind of shower gel. For glue specimen at its liquid phase, we measure the value of tan _ decreases from about 103 at 0.01 Hz to 1 at 100 Hz. For hardened glue, its loss tangent is about 0.5 to 0.05 between 0.01 and 100 Hz. In addition, a machine deep learning method is proposed to analyze the particle size and its distribution in colloidal suspensions.

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