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研究生: 黃安妮
Huang, Anny
論文名稱: 異金屬(3d-4f)配位聚合物的合成、結構鑑定與磁性行為
Synthesis,Crystal Structure and Magnetic Behavior of Heterometallic 3d-4f Coordination polymers
指導教授: 許桂芳
Hsu, Kuei-Fang
學位類別: 碩士
Master
系所名稱: 理學院 - 化學系
Department of Chemistry
論文出版年: 2009
畢業學年度: 97
語文別: 中文
論文頁數: 99
中文關鍵詞: 水熱異金屬
外文關鍵詞: heterometallic, hydrothermal
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  • 利用水熱溶劑熱法,我們成功的合成出一系列鑭金屬和銅金屬的異金屬化合物。我們實驗得到七個3d-4f異金屬化合物。化合物先經由單晶X-光繞射儀定出化合物的結構,元素分析儀確定化合物的純度,紅外線光譜儀分析特定官能基,並利用超導磁性量子干涉儀探討其磁性行為。

    The assembly of heterometallic 3d-4f ions and organic ligands has successfully constructed a series of metal-organic frameworks by the hydrothermal reactions. Single-crystal structures, elemental analyses, infrared records, and magnetic behavior were characterized for these compounds.
    along the a axis.

    目錄 摘要 i 謝誌 iv 目錄 v 表目錄 vii 圖目錄 x 第一章 緒論 12 1-1 研究緣由 12 第二章 化合物1之合成、結果與討論 21 2-1 合成條件 24 2-2 單晶X-光繞射分析 28 2-3 結果討論 32 2-3-1 化合物1晶體結構解析 34 2-3-2 化合物1磁性測量 45 第三章化合物2之合成、結果與討論 48 3-1 合成條件 48 3-2 單晶X-光繞射分析 49 3-3 結果討論 50 3-3-1 化合物2晶體結構解析 51 3-3-2 化合物2磁性測量 63 結論 64 參考文獻 66 附錄 69

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